Determination of volatile organic compounds in Kazakhstan red wine by headspace solid-phase microextraction in combination with GC-MS

DOI: https://doi.org/10.15328/chemb_2013_4152-161
Keywords: Red Wine, HS-SPME, GC-MS, Volatile Organic Compounds

Abstract

An analytical method for determination of volatile organic compounds (VOCs) in Kazakhstan red wine was developed in this study. The volatile composition of red wine was determined by headspace SPME in combination with GC-MS. The DVB/CAR/PDMS fiber and the sample volume of 10 mL were chosen. The optimal conditions for HS-SPME were temperature of 30°C and extraction time of 60 s. Addition of 3 g NaCl and no pH adjusting were the most suitable parameters for extraction of VOCs from wine. The developed methodology enables to identify compounds referring to the following classes such as esters, alcohols, aldehydes, acids, ketones and naphthalenes and can be applied for forensic examination of Kazakhstan red wine.

Author Biographies

Ainur Utesheva, al-Farabi Kazakh National University
Center of Physical Chemical Methods of Research and Analysis
Meruert Sergazina, al-Farabi Kazakh National University
Center of Physical Chemical Methods of Research and Analysis
Mereke Alimzhanova, al-Farabi Kazakh National University
Center of Physical Chemical Methods of Research and Analysis
Bulat Kenessov, al-Farabi Kazakh National University
Center of Physical Chemical Methods of Research and Analysis

References

1 "Interfax.kz" Internet newspaper 15 Dec. (2009) Wine consumption in the world will grow at the expense of Asia. http://www.meta.kz/351588-potreblenie-vina-v-mire-budet-rasti-za-schet-azii.html. (In Russian)

2 Internet newspaper (2002) Wine consumption in Kazakhstan. http://www.tns-global.kz/ru/publication/publ74.php. (In Russian)

3 Andujar-Ortiz I, Moreno-Arribas MV, Martín-Álvarez PJ, MA Pozo-Bayón (2009) J Chromatogr A 1216:7351–7357. http://dx.doi.org/10.1016/j.chroma.2009.08.055

4 Antalick G, Perello MC, Gilles de Revel (2012) Food Chemi 121:1236-1245. http://dx.doi.org/10.1016/j.foodchem.2010.01.011

5 Barros EP, Moreira N, Pereira GE, Selma Gomes Ferreira Leite; Claudia Moraes Rezende; Paula Guedes de Pinho (2012) Talanta 101:177-186. http://dx.doi.org/10.1016/j.talanta.2012.08.028

6 Setkova L, Risticevic S, Pawliszyn J (2007)  J Chromatogr A 1147:213-223. http://dx.doi.org/10.1016/j.chroma.2007.02.058

7 Gómez Gallego MA, García-Carpintero EG, Sánchez-Palomo E,  Gonzalez Viñas MA, Hermosín-Gutiérrez I (2012) Food Chem 134:851-863. http://dx.doi.org/10.1016/j.foodchem.2012.02.194

8 Silva LR, Andrade PB , Valentao P, Seabra RM, TrujilloME, Encarna Velazquez (2005) Food Chem 89:185–189 http://dx.doi.org/10.1016/j.foodchem.2004.02.019

9 S. M. Rodrigues; M. Otero; A. A. Alves; J. Coimbra;M. A. Coimbra; E. Pereira; A. C. Duarte. Elemental analysis for categorization of wines and authentication of their certified brand of origin // Journal of Food Composition and Analysis – 2011 - #24 – P. 548–562

10 A. E. Martin; R. J. Watling; G. S. Lee. The multi-element determination and regional discrimination of Australian wines // Food Chemistry – 2012 - #133 – P. 1081–1089

 

Published
2013-09-14
How to Cite
Utesheva, A., Sergazina, M., Alimzhanova, M., & Kenessov, B. (2013). Determination of volatile organic compounds in Kazakhstan red wine by headspace solid-phase microextraction in combination with GC-MS. Chemical Bulletin of Kazakh National University, 72(4), 152-161. https://doi.org/https://doi.org/10.15328/chemb_2013_4152-161
Issue
Vol 72 No 4 (2013): Chemical Bulletin of Kazakh National University
Section
Analytical Chemistry
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