Karachaganak field – innovational method of direct determination of saturates–waxes–aromatics– resins–asphaltens by TLC-FID technique

  • F. Germi Production Chemical Laboratory, Karachaganak Petroleum Operating b.v., Aksai
  • B. Gabdushev Production Chemical Laboratory, Karachaganak Petroleum Operating b.v., Aksai
  • T. Zakiyev Production Chemical Laboratory, Karachaganak Petroleum Operating b.v., Aksai

Abstract

Based on separation of fluid compounds on the thin bonded layer of absorber (the stationary phase is a Chromarods – quartz rod with a silica surface) by means of the selective solvents (mobile phase) combined with technique of ionization of separated compounds by Flame Ionization Detector (FID), the KPO b.v. Chemical Laboratory could achieve direct separation of crude oil sample in one run into 5 compounds qualified as SWARA (Saturated–Waxes–Aromatics–Resins– Asphaltenes).

References

1. IP 469/D1 (2006), Determination of saturated, aromatics and polar compounds in petroleum products by thin layer chromatography and flame ionization detector.
2. A New Test Method for Determination of Wax Contenet in Cruid Oils, Residues and Bitumens. Xiaohu Lu, Bjorn Kalman, Per Redelius. ―AB Nynas Petroleum, Bitumen Research‖ , ―Swedish National Road and Transport Research Institute (VTI)‖
3. Improved Sample Application Methods for the Iatroscan. H. READ, BP Research Center, Chertsey Road, Sunbury on Thames, Middlesex, TW167LN. England.
4. Thin Layer Chromatography – Flame Ionization Detection. Analysis of IN–SITU petroleum biodegradation. Frank L. Stephens. August 2004.
5. A new North Sea oil–based standard for Iatroscan analysis. Sunil Bharat, Richard Patience, Nigel Mills and Trond Hanesand.
6. Alternative calibration and standardization procedure of Iatroscan TLC–FID for SARA hydrocarbon class quantification: Application to TAR–MAT zone identification. Miguel Orea, Margarita Alberti, Armando Ruggiero, and Silvia Colaiocco.
Published
2011-03-30
How to Cite
Germi, F., Gabdushev, B., & Zakiyev, T. (2011). Karachaganak field – innovational method of direct determination of saturates–waxes–aromatics– resins–asphaltens by TLC-FID technique. Chemical Bulletin of Kazakh National University, 61(1), 223-229. Retrieved from https://bulletin.chemistry.kz/index.php/kaznu/article/view/903
Issue
Vol 61 No 1 (2011): Chemical Bulletin of Kazakh National University
Section
Other Papers

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